There are many applications for high purity fluids (gases and liquids) delivered from vessels (e.g., tanks and cylinders). Such high-purity fluids are often used in processing of electronic, optical, pharmaceutical and chemical products.
In some cases, it is advantageous to purify these fluids at the time they are withdrawn from said vessels, particularly since storage in the vessel can often impart impurities to the fluid over time. Purification can be accomplished by passing the fluid through a purification media such as adsorbents, getters or filters.
A useful means of accomplishing this purification is to situate an inner vessel containing the purification medium within the interior of the vessel that contains the fluid; the inlet of the inner vessel would be in fluid communication with the interior volume of the outer vessel.
Some purification media, however, can have the paradoxical ability to add contaminants to the fluid that they are intended to purify. One specific example is the case where the purification medium acts as a decomposition catalyst for the fluid being purified.
In many cases, the rate at which this decomposition occurs rises monotonically with the pressure of the fluid, particularly if the fluid is compressible (i.e. when it is a gas).
In a different example, some media are known to slowly leach or desorb contaminants into the fluid.
These problems are overcome by the present invention wherein contamination of the small amount of fluid in direct contact with the purification media within the inner vessel may be tolerable, as long as this contamination is minimized and not allowed to diffuse or otherwise mix with the bulk of the fluid stored in the outer vessel. For instance, using the present invention, it may be possible to briefly vent the small amount of contaminated fluid in the inner vessel before using the contents in the application that requires high purity. These and other advantages of the present invention will be set forth in greater detail below.